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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 633618Generated: October 31, 2026

Trifluoroacetic acid → HCID 71203152, compound

https://huagongshe.com/reaction/633618

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 71186588HCID 71186588—
SolventDichloromethaneHCID 6344—
ProductHCID 71203152HCID 71203152—

Reaction Steps

55 μl of trifluoroacetic acid were added to a solution of 39 mg of tert-butyl {-4-[5-(2,5-difluorophenoxy)-7-propyloxazolo[5,4-d]pyrimidin-2-yl]-2,6-dimethylphenoxy}acetate in 0.4 ml of dichloromethane, and the mixture was stirred at room temperature for 16 h. The reaction was then concentrated under reduced pressure, and the residue was triturated with diisopropyl ether, filtered off with suction and dried. This gave 21 mg (60%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09321787B2
Source datasetuspto-grants-2016_04
ORD IDord-3e39ee784a6e47efa14faa5f537aa9d6
Source noteuspto-grants-2016_04