HCID 178490493, compound → HCID 178489872, compound

Participants

Reaction Steps

40 g of N-[2-(4-chlorobenzyl)-4,6-dihydroxypyrimidin-5-yl]-4-methoxy-3,5-dimethylbenzamide and 150 ml of phosphorus oxychloride were heated at 70° C. for 1.5 h. The mixture was then allowed to cool. The solid formed was filtered off with suction, washed with diethyl ether and dried. This gave 21.1 g (55%) of the title compound.

Provenance & Evidence