反应详情

温度

100 °C

Synthesis of 2-(2-methyl-6-(tetrahydrofuran-3-yl)phenoxy)acetohydrazide: methyl 2-(2-methyl-6-(tetrahydrofuran-3-yl)phenoxy)acetate (141 mg, 0.56 mmol) and hydrazine (0.03 mL, 0.6 mmol) were dissolved in EtOH 2 mL, followed by stirring at 100° C. for 12 hours. After the completion of the reaction, the reaction mixture was concentrated under reduced pressure to obtain 2-(2-(furan-3-yl)-6-methylphenoxy)acetohydrazide (127 mg, 90%).

1. customAfter the completion of the reaction
2. concentrationthe reaction mixture was concentrated under reduced pressure