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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 63369Generated: October 30, 2026

Hydrazine → HCID 90002256, compound

https://huagongshe.com/reaction/63369

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazineHCID 9321—
ReactantHCID 90002242HCID 90002242—
Reactant2-(2-Methyl-6-(tetrahydrofuran-3-yl)phenoxy)acetohydrazideHCID 90002699—
SolventEthanolHCID 702—
ProductHCID 90002256HCID 9000225690%

Reaction Conditions

Temperature100 °C

Reaction Steps

Synthesis of 2-(2-methyl-6-(tetrahydrofuran-3-yl)phenoxy)acetohydrazide: methyl 2-(2-methyl-6-(tetrahydrofuran-3-yl)phenoxy)acetate (141 mg, 0.56 mmol) and hydrazine (0.03 mL, 0.6 mmol) were dissolved in EtOH 2 mL, followed by stirring at 100° C. for 12 hours. After the completion of the reaction, the reaction mixture was concentrated under reduced pressure to obtain 2-(2-(furan-3-yl)-6-methylphenoxy)acetohydrazide (127 mg, 90%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09447083B2
Source datasetuspto-grants-2016_09
ORD IDord-1bbfb45c28f84f6cbc642f992f912dc3
Source noteuspto-grants-2016_09