HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 131735475, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 1-[6-(2-Fluoroethoxy)-3-pyridinyl]ethanone | HCID 58629025 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 131735475 | HCID 131735475 | — |
Reaction Steps
362 mg (1.98 mmol) of 1-[6-(2-fluoroethoxy)pyrid-3-yl]ethanone, 413 μl (7.61 mmol) of hydrobromic acid, 537 μl (9.88 mmol) of bromine and 5 mL of glacial acetic acid were used in the reaction. After precipitation with ethyl ether and filtration, 602 mg of 2-bromo-1-[6-(2-fluoroethoxy)pyrid-3-yl]ethanone hydrobromide are obtained, the characteristics of which are as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09321790B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-87df87d8c7344fab8c9ce21cedeeb4d3 |
| Source note | uspto-grants-2016_04 |