HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 118131246, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | HCID 118131269 | HCID 118131269 | — |
| Product | HCID 118131246 | HCID 118131246 | 38.9% |
Reaction Steps
The title compound was made in a similar way of that of Intermediate B53 from 4-bromo-7-chloro-3-(1-hydroxyethyl)-1H-isochromen-1-one (intermediate A5, 1.4 g, 4.61 mmol) and phenylboronic acid (0.844 g, 6.92 mmol) to afford title compound as a yellow foam (0.540 g) which was used without any additional purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09321776B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-da99c91a399e43a99a242eb1a5f7d68d |
| Source note | uspto-grants-2016_04 |