HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 118131321, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | HCID 118131311 | HCID 118131311 | — |
| Product | HCID 118131321 | HCID 118131321 | 45% |
Reaction Steps
The title compound was made in a similar way of that of Intermediate B53 from 4-bromo-6-chloro-3-(1-hydroxyethyl)-1H-isochromen-1-one (intermediate A6, 0.973 g, 3.205 mmol) and phenylboronic acid (0.586 g, 4.808 mmol) to yield title compound as a white foam (0.430 g, 1.43 mmol, 45%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09321776B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-3da013b1392343a7bab7405e039e7dab |
| Source note | uspto-grants-2016_04 |