HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 118131122, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | HCID 118131055 | HCID 118131055 | — |
| Product | HCID 118131122 | HCID 118131122 | 78.2% |
Reaction Steps
The title compound was made in a similar way of that of Intermediate B53 from 4-bromo-6-fluoro-3-(1-hydroxyethyl)-1H-isochromen-1-one (intermediate A7, 0.95 g, 3.31 mmol) and phenylboronic acid (0.605 g, 4.96 mmol) to afford title compound (0.736 g) which was used without any additional purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09321776B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-7ee30bbedbc84e44b306a0b4c482d824 |
| Source note | uspto-grants-2016_04 |