HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 178424545, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-(1-Bromoethyl)-4-m-tolyl-1H-isochromen-1-one | HCID 118131032 | — |
| Reactant | HCID 178519204 | HCID 178519204 | — |
| Reactant | HCID 178527205 | HCID 178527205 | — |
| Product | HCID 178424545 | HCID 178424545 | 87% |
Reaction Steps
The title compound was made in a similar way as that of the compound of example 10, 3-(1-bromoethyl)-4-m-tolyl-1H-isochromen-1-one (intermediate C5, 67 mg, 0.195 mmol), 9H-purine-6-thiol hydrate (33.2 mg, 0.195 mmol)) and K2CO3 (27 mg, 0.111 mmol) to give to give the title compound (70 mg, 87%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09321776B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-9bb4d5169ba741929e95dbe9a342b3be |
| Source note | uspto-grants-2016_04 |