HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethoxyaniline → HCID 178420283, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethoxyaniline | HCID 9076 | — |
| Reactant | 4-(4-Benzyloxyphenyl)cyclohexanone | HCID 21260493 | — |
| Reactant | HCID 178420282 | HCID 178420282 | — |
| Product | HCID 178420283 | HCID 178420283 | 15% |
Reaction Steps
Following the general method of example 3, cis-[4-(4-benzyloxy-phenyl)-cyclohexyl]-phenethyl-amine, (260 mg; 11% light yellow oil, MS: m/e=386.2 (M+H+)) trans-[4-(4-benzyloxy-phenyl)-cyclohexyl]-phenethyl-amine (370 mg; 15 % white crystals, MS: m/e=386.3 (M+H+)) were prepared from 4-(4-benzyloxy-phenyl)-cyclohexanone (1.8 g; 6.4 mmol) and phenetylamine (0.78 g; 6.4 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06184236B2 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-fbde65fb161a41029f71c3d35e65fafa |
| Source note | uspto-grants-2001_02 |