HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylpropylamine → HCID 178420266, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylpropylamine | HCID 16259 | — |
| Reactant | 4-(4-Benzyloxyphenyl)cyclohexanone | HCID 21260493 | — |
| Reactant | HCID 178420265 | HCID 178420265 | — |
| Product | HCID 178420266 | HCID 178420266 | 30% |
Reaction Steps
Following the general method of example 3, cis-[4-(4-benzyloxy-phenyl)-cyclohexyl]-(3-phenyl-propyl)-amine, (710 mg; 17% light yellow oil, MS: m/e=400.4 (M+H+)) trans-[4-(4-benzyloxy-phenyl)-cyclohexyl]-(3-phenyl-propyl)-amine (1.26 g; 30% white crystals, MS: m/e=400.4 (M+H+)) were prepared from 4-(4-benzyloxy-phenyl)-cyclohexanone (3.0 g; 10.7 mmol) and 3-phenyl-propylamine(1.45 g; 10.7 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06184236B2 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-bbcfa144d06f42969cb801f2d7e63091 |
| Source note | uspto-grants-2001_02 |