HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenepropanoic acid → N-(2-hydroxy-1-hydroxymethyl-ethyl)-3-phenyl-propionamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenepropanoic acid | HCID 107 | — |
| Reactant | Serinol | HCID 68294 | — |
| Product | N-(2-hydroxy-1-hydroxymethyl-ethyl)-3-phenyl-propionamide | HCID 21260455 | — |
Reaction Steps
The procedure of example 79c was followed, using 3-phenylpropionic acid and serinol. At the end of the reaction, the DMF was evaporated and CH2Cl2 was added to the residue. The white crystalline material was collected and gave pure N-(2-hydroxy-1-hydroxymethyl-ethyl)-3-phenyl-propionamide as a white solid (56%, MS: m/e=224.2 (M+H+)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06184236B2 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-0816cec434254e5dbd036649f0c91b12 |
| Source note | uspto-grants-2001_02 |