Tetrahydrothiophene → HCID 53921306, compound
Reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([SH:8])=[CH:4][CH:3]=1.[S:9]1[CH2:13][CH2:12][CH2:11][CH2:10]1>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][CH:11]2[CH:12]([S:8][C:5]3[CH:6]=[CH:7][C:2]([Cl:1])=[CH:3][CH:4]=3)[CH:13]([C:10]3[S:9][CH:13]=[CH:12][CH:11]=3)[S:9][CH:10]2[C:10]2[S:9][CH:13]=[CH:12][CH:11]=2)=[CH:4][CH:3]=1Participants
3
Procedure
Starting from 4-chlorothiophenol, the synthesis of this compound is analogous to that of the tetrahydrothiophene synthesized in Example 2.
Workup
- customthe synthesis of this compound
Sources & evidence
- ORD record
- ord-3638b3161406419f8b492cc2ee3c6fd0
- Source dataset
- uspto-grants-2001_02
- Patent number
- US06184540B2
Reaction notes
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