HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Chlorophenyl)piperazine → HCID 17773079, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Chlorophenyl)piperazine | HCID 97478 | — |
| Reactant | 4-(4-Chlorophenyl)piperidine | HCID 1203613 | — |
| Reactant | 3-(4,5,6,7-tetrahydro-2H-indazol-3-yl)propanoic acid | HCID 178525369 | — |
| Product | HCID 17773079 | HCID 17773079 | — |
Reaction Steps
In the same manner as in Example 102 except that 3-(2-(4-chlorophenyl)-4,5,6,7-tetrahydro-2H-indazol-3-yl)propionic acid obtained in Starting Material Synthesis Example 12 and 1-(4-chlorophenyl)piperazine were used instead of 3-(4,5,6,7-tetrahydro-2H-indazol-3-yl)propionic acid obtained in Starting Material Synthesis Example 1 and 4-(4-chlorophenyl)piperidine, 2-(4-chlorophenyl)-3-(3-(4-(4-chlorophenyl)piperazin-1-yl)propyl)-4,5,6,7-tetrahydro-2H-indazole was obtained, m.p. 129-131° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06187774B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-c303993aaabf4952885b807ad68642d5 |
| Source note | uspto-grants-2001_02 |