HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Methoxy-5-nitrophenyl)ethanone → 1-(5-Amino-2-methoxyphenyl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Methoxy-5-nitrophenyl)ethanone | HCID 18615104 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | 1-(5-Amino-2-methoxyphenyl)ethanone | HCID 15579443 | — |
Reaction Steps
The above-identified compound (2.13 g) was obtained by processing Intermediate 72 (2.50 g) through reaction and after-treatment in accordance with the procedures of the step C of Example 63. Rf=0.38 (methanol/chloroform of 1/19).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06187809B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-d1d4db27cd774808a4fd133d5ce6000b |
| Source note | uspto-grants-2001_02 |