HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 15382693, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 4-Nitrobenzoyl chloride | HCID 8502 | — |
| Reactant | N-benzoyl-2'-deoxyadenosine | HCID 107558 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 15382693 | HCID 15382693 | — |
Reaction Steps
The synthesis of this product is carried out by reacting 1 eq of p-nitrobenzoyl chloride with 6-N-benzoyldeoxyadenosine for 4 hours in pyridine. After hydrolysis of the excess reagent, partial evaporation of the pyridine, extraction and evaporation of the chloroformic phase, the product is obtained by column chromatography (elution 4% methanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06187914B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-5abaca9d871242a3abe42dc791ab9001 |
| Source note | uspto-grants-2001_02 |