huagongshe.com
HRID635500

反应详情

EQUATION

反应方程式

HRID 635500 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)c1ccc([N+](=O)[O-])cc1
HCID8502

4-Nitrobenzoyl chloride

C7H4ClNO3

结构：CC(C)C(=O)Nc1nc2c(ncn2[C@H]2C[C@H](O)[C@@H](CO)O2)c(=O)[nH]1
HCID135407017

Guanosine, 2'-deoxy-N-(2-methyl-1-oxopropyl)-

C14H19N5O5

PRODUCTS

生成物

1
结构：CC(C)C(=O)Nc1nc2c(ncn2[C@H]2C[C@H](O)[C@@H](COC(=O)c3ccc([N+](=O)[O-])cc3)O2)c(=O)[nH]1
HCID137182964

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

The synthesis of this product is carried out by reacting 1.1 eq of p-nitrobenzoyl chloride with 2-N-isobutyryldeoxyguanosine for 16 hours in pyridine. After extraction with a dichloromethane/sodium bicarbonate mixture and evaporation to dryness, the product is taken up in chloroform. This product was not used because it was too insoluble.

WORKUP

后处理

  1. customThe synthesis of this product
  2. customfor 16 hours
  3. extractionAfter extraction
  4. customwith a dichloromethane/sodium bicarbonate mixture and evaporation to dryness