HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dichloroethane → HCID 86756417, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dichloroethane | HCID 6365 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 69978536 | HCID 69978536 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 86756417 | HCID 86756417 | — |
Reaction Steps
93 mg of triethylamine was added to a mixture comprising 0.30 g of α-(2,4-dichlorophenyl)-β-hydroxy-β-(2-trifluoromethylphenyl)acrylonitrile and 7 ml of dichloroethane. Then, 96 mg of methanesulfonyl chloride was added thereto, and the mixture was reacted for 17 hours at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06187944B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-b230da4b18f440b294a1d8f3df50d5fe |
| Source note | uspto-grants-2001_02 |