HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dichloroethane → HCID 86756418, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dichloroethane | HCID 6365 | — |
| Reactant | 1-Propanesulfonyl chloride | HCID 66279 | — |
| Reactant | HCID 69976425 | HCID 69976425 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 86756418 | HCID 86756418 | — |
Reaction Steps
60 mg of triethylamine was added to a mixture comprising 0.20 g of α-(4-bromophenyl)-β-hydroxy-β-(2-trifluoromethylphenyl)acrylonitrile and 6 ml of dichloroethane. Then, a mixture comprising 77 mg of n-propanesulfonyl chloride and 2 ml of dichloroethane, was dropwise added thereto. After completion of the dropwise addition, the mixture was reacted for 15 hours at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06187944B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-15ea409c747845998c44820429260939 |
| Source note | uspto-grants-2001_02 |