Hydrochloric Acid → HCID 21259553, compound

Participants

Reaction Steps

An aqueous solution of 3.04 g (9.90 mmol) of tris(3-aminophenyl)phosphine in 100 ml of water was treated with 13.5 ml of hydrochloric acid (2 N) and the clear solution was stirred at room temperature for 30 minutes. The solvent was distilled off at 60° C. under reduced pressure, giving 3.21 g of tris(3-ammoniophenyl)phosphine trichloride as a colorless solid (yield: 78%).

Provenance & Evidence