HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium methanethiolate → HCID 21256517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium methanethiolate | HCID 4378561 | — |
| Reactant | HCID 21256546 | HCID 21256546 | — |
| Solvent | N,N-dimethylformamide methanol | HCID 21901440 | — |
| Product | HCID 21256517 | HCID 21256517 | 53% |
Reaction Steps
586 mg of 2-(2-bromoethyl)-1,4-benzoxazin-3-one is mixed in a methanol-DMF mixture with 245 mg of sodium thiomethylate while being stirred. After 4 hours, it is concentrated by evaporation. After column chromatography, the title compound is obtained in a yield of 53%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06191127B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-1c5483c1d4504eeb98cae5c3f09a9778 |
| Source note | uspto-grants-2001_02 |