HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178428562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Chloro-4-methylpyrimidine | HCID 11629607 | — |
| Reactant | HCID 178521570 | HCID 178521570 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178428562 | HCID 178428562 | — |
Reaction Steps
The compound 10a (4.3 g, 23.3 mmol) is placed in 100 ml of toluene in the presence of 2-chloro-4-methylpyrimidine (3 g, 23.3 mmol) and of triethylamine (4.9 ml, 35.1 mmol) and then this mixture is heated at reflux for 16 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06191130B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-3c057c410ef8429f9e6d1857a2996c85 |
| Source note | uspto-grants-2001_02 |