Aluminium lithium hydride → HCID 467125, compound

Participants

Reaction Steps

3-(2-Furanyl)-1-(6,7,8,9-tetrahydro-5H-cyclohept[d]imidazo[2,1-b]thiazol-3-yl)-propene-1-one (Formula P-2, X=0), 0.94 g, was reduced with LiAlH4 by non-critical variations of EXAMPLE 23 to provide α-[2-(2-Furanyl)ethyl]-6,7,8,9-tetrahydro-5H-cyclohept[d]imidazo[2,1-b]thiazol-3-methanol (Formula P-5, X=0), after two crystallizations from ethanol.

Provenance & Evidence