反应详情

Indene (10.0 g, 0.0861 moles) was stirred in hexane (150 mL) as n-BuLi (0.8783 moles, 54.8 mL of 1.6 M solution in hexane) was added drop wise. The mixture was allowed to stir overnight at room temperature during which time a solid precipitated. After the reaction period the solid was collected via suction filtration, washed with hexane, dried under vacuum, and was used without further purification or analysis (9.35 g, 89.1% yield).

1. additionwas added drop wise
2. customprecipitated
3. customAfter the reaction period the solid
4. filtrationwas collected via suction filtration
5. washwashed with hexane
6. customdried under vacuum
7. customwas used without further purification or analysis (9.35 g, 89.1% yield)