HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 21257363, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 85782707 | HCID 85782707 | — |
| Product | HCID 21257363 | HCID 21257363 | 90% |
Reaction Steps
Compound 10 (19 g, 71.69 mmol) was treated with Conc. H2SO4 (48 mL, 901 mmol) for 30 min. as described for II after usual work up afforded 5,7-dimethoxy-4-propyl-1,2-dihydro-2-quinolinone (12,159) in 90% yield as a white solid. M.P. 193-196° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06191279B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-b24a8f07793d47fba89a6c931d03baab |
| Source note | uspto-grants-2001_02 |