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HRID636196

反应详情

EQUATION

反应方程式

HRID 636196 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)[C@@H](N)Cc1ccc(O)cc1
HCID70364

L-Tyrosine, ethyl ester

C11H15NO3

结构：C[C@H](NC(=O)Cc1cccc([N+](=O)[O-])c1)C(=O)O
HCID53788870

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)[C@H](Cc1ccc(O)cc1)NC(=O)[C@H](C)NC(=O)Cc1cccc([N+](=O)[O-])c1
HCID9824664

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Following General Procedure C and using N-(3-nitrophenylacetyl)-L-alanine (prepared from 3-nitrophenylacetic acid (Aldrich) and L-alanine ethyl ester hydrochloride (Sigma) using General Procedure C, followed by hydrolysis using General Procedure AF) and L-tyrosine ethyl ester (Sigma), the title compound was prepared as a solid (mp=117-119° C.). The reaction was monitored by tlc (Rf=0.5 in EtOAc) and the product was purified by silica gel chromatography using EtOAc as the eluent.

WORKUP

后处理

  1. customthe product was purified by silica gel chromatography