HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69910017, compound → HCID 54295887, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69910017 | HCID 69910017 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54295887 | HCID 54295887 | — |
Reaction Steps
A suspension of 1′-amino-3′, 5′, 5-tris(methoxybenzyl) thymidine and 10% palladium on charcoal in ethanol is shaken in a hydrogenation apparatus under hydrogen pressure of 50 psi for 24 h. The solid is filtered and the filtrate concentrated. The crude is purified by recrystallization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06191266B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-2c6354398c1e45b9ac22f1f482daa0b8 |
| Source note | uspto-grants-2001_02 |