HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl piperidine-2-carboxylate → HCID 70235600, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl piperidine-2-carboxylate | HCID 27517 | — |
| Reactant | 1,3-Thiazole-5-carbonyl chloride | HCID 22458141 | — |
| Product | HCID 70235600 | HCID 70235600 | — |
Reaction Steps
Ethyl N-(5-thiazolylcarbonyl)pipecolinate is prepared as in Example 1, from 4.4 g of ethyl pipecolinate and 5.25 g of 5-chloroformylthiazole. 7.7 g of ethyl N8(5-thiazolylcarbonyl)pipecolinate are thus obtained in the form of brown oil. (Rf=0.51; thin layer chromatography on silica gel; eluent: 55/45 dichloromethane/ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06194426B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-5bbf1ed3df1c44bfbe7c2709a0c6d8d9 |
| Source note | uspto-grants-2001_02 |