HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Acetyl-2,7-dichloro-3-(3-pyridyl)-5,6-dihydroindolizine → HCID 21255146, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Acetyl-2,7-dichloro-3-(3-pyridyl)-5,6-dihydroindolizine | HCID 22012136 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 21255146 | HCID 21255146 | 3.3% |
Reaction Steps
1-Acetyl-2-chloro-3-(3-pyridyl)-5,6,7,8-tetrahydroindolizine is prepared as described in Example 39, from 1.7 g of 1-acetyl-2,7-dichloro-3-(3-pyridyl)-5,6-dihydroindolizine and from 0.09 g of 10% palladium on charcoal. 0.05 g of 1-acetyl-2-chloro-3-(3-pyridyl)-5,6,7,8-tetrahydroindolizine are thus obtained in the form of whitish crystalline solid melting at 115° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06194426B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-55f2b2144f9540b9af75cd4195452d90 |
| Source note | uspto-grants-2001_02 |