Ethanol → HCID 22611021, compound

Participants

Reaction Steps

A mixture of 2-nitro-N-(4-(2-thiazolylamino)phenyl)aniline (1.2 g, 3.8 mmol), sodium sulfide nona hydrate (4.61, 19.2 mmol), ammonium chloride (1.03 g, 19.2 mmol) and ethanol (40 ml) was stirred at reflux for 40 h. Water (50 ml) was added, the mixture was stirred an d filtered. Yield 0.49 g, 46%. M.p. 184-186° C.

Provenance & Evidence