Tert-Butylamine → HCID 21255693, compound

Participants

Reaction Steps

To a solution of 2,4-difluorobenzaldehyde (431.6 mg, 3.04 mmol) in toluene (5 ml) was added t-butylamine (0.63 ml, 6.00 mmol) and stirred under reflux using a Dean-Stark trap to remove water for 1 hour. Then t-butylamine (0.63 ml, 6.00 mmol) was added to the mixture and stirred for 5 hours. The solvent was evaporated to give the title compound.

Provenance & Evidence