4-Aminocyclohexanol → HCID 86756473, compound

HRID 636789Notes

Reaction equation

HRID 636789 reaction equation
[C:1]1([S:11]([Cl:14])(=[O:13])=[O:12])[CH:6]=[CH:5][C:4]([S:7]([Cl:10])(=[O:9])=[O:8])=[CH:3][CH:2]=1.[NH2:15][CH:16]1[CH2:21][CH2:20][CH:19]([OH:22])[CH2:18][CH2:17]1>C1N2CCN(CC2)C1>[NH2:15][CH:16]1[CH2:21][CH2:20][CH:19]([OH:22])[CH2:18][CH2:17]1.[C:1]1([S:11]([Cl:14])(=[O:12])=[O:13])[CH:2]=[CH:3][C:4]([S:7]([Cl:10])(=[O:8])=[O:9])=[CH:5][CH:6]=1

Participants

4

Reactant 2

HCID 812934-AminocyclohexanolHCID 21255763Benzene-1,4-disulfonyl dichloride2×

Product 1

HCID 86756473HCID 86756473, compound

Reagents, catalysts & solvents 1

HCID 9237DabcoCatalyst

Procedure

Next, in the mixing section 22, the vapor of 1,4-benzenedisulfonyl chloride was cooled, and the introduced base particles were exposed thereto for 10 minutes. Consequently, a polymerization reaction using triethylenediamine as a catalyst took place on the surface of the base particles between 4-aminocyclohexanol and 1,4-benzenedisulfonyl chloride, forming a film of 4-aminocyclohexanol-1,4-benzenedisulfonyl chloride co-polymer.

Workup

  1. customConsequently, a polymerization reaction

Sources & evidence

ORD record
ord-69a5ea8bc810413f88907fd21617d099
Source dataset
uspto-grants-2001_02
Patent number
US06194487B1

Reaction notes

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