Glycerol → HCID 86756478, compound

HRID 636795Notes

Reaction equation

[C:1]([Cl:12])(=[O:11])[C:2]1[CH:10]=[CH:9][CH:8]=[C:4]([C:5]([Cl:7])=[O:6])[CH:3]=1.[OH-].[Na+].[OH:15][CH2:16][CH:17]([CH2:19][OH:20])[OH:18]>>[OH:15][CH2:16][CH:17]([CH2:19][OH:20])[OH:18].[C:5]([Cl:7])(=[O:6])[C:4]1[CH:8]=[CH:9][CH:10]=[C:2]([C:1]([Cl:12])=[O:11])[CH:3]=1

Participants

Reactant 3

HCID 753Glycerol

HCID 7451Isophthaloyl chloride2×

HCID 14798Sodium Hydroxide

Product 1

HCID 86756478HCID 86756478, compound

Procedure

Next, in the mixing section 22, the vapor atmosphere of isophthaloyl chloride was cooled, and the introduced base particles were exposed thereto for 3 minutes. Consequently, a polymerization reaction, using as a catalyst sodium hydroxide contained in the base particles, took place on the surface of the base particles between glycerol and isophthaloyl chloride, forming a film of glycerol-isophthaloyl chloride co-polymer.

Workup

customConsequently, a polymerization reaction

Sources & evidence

ORD record: ord-a0465e3a2e3e452f9105a754461ee005
Source dataset: uspto-grants-2001_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06194487B1

Reaction notes

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