HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylpiperidine-1-sulfonyl chloride → HCID 70225375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylpiperidine-1-sulfonyl chloride | HCID 16228446 | — |
| Reactant | HCID 70224708 | HCID 70224708 | — |
| Product | HCID 70225375 | HCID 70225375 | 93.1% |
Reaction Steps
According to the procedure of Example 13, 4-{[1-(3-aza-bicyclo[3.1.0]hex-6-yl)-5-oxo-4,4-bis-pyridin-4-ylmethyl-imidazolidin-2-ylidene]-acetyl}-benzonitrile (50 mg, 0.102 mmol) and 4-methyl-piperidine-1-sulfonyl chloride (60.2 mg, 0.306 mmol) were reacted to generate the title compound as an off-white solid (62 mg, 0.095 mmol, 93% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06194438B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-a445547961fa438789ca688dd94df9be |
| Source note | uspto-grants-2001_02 |