HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18465020, compound → HCID 18464884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18465020 | HCID 18465020 | — |
| Reactant | 4-(1-(2-ethoxyethyl)-1H-benzimidazol-2-yl) [1,4]diazepane hydriodic acid salt | HCID 86583887 | — |
| Product | HCID 18464884 | HCID 18464884 | — |
Reaction Steps
Prepare by the method of Example 7.6 using 1-(2-methoxybenzyl)-3-(3 5-di(trifluoromethyl)phenylmethyl)-3-(2-methanesulfonyloxyethyl)-2-oxopyrrolidine and 4-(1-(2-ethoxyethyl)-1H-benzimidazol-2-yl)[1,4]diazepane hydriodic acid salt to give the title compound: Rf=0.54 (silica gel, 5% methanol/dichloromethane/0.5% concentrated aqueous ammonia).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06194406B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-f7a3ad18eacc464aace07c87a9251cc8 |
| Source note | uspto-grants-2001_02 |