HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 53638471, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 15591551 | HCID 15591551 | — |
| Product | HCID 53638471 | HCID 53638471 | — |
Reaction Steps
In a 250 ml round-bottomed flask, (S)-3-[N-(α-methylbenzyl)-carbamoyl]-5-chloromethyl-2,6-dimethylpyridine (21 g), the preparation of which is described in Example 6, is introduced into anhydrous methanol (50 ml). After dissolution, a solution of sodium (5.00 g) in methanol (50 ml) is run in.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04556414 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-5338aea264ad49458703a72c48a99cfd |
| Source note | uspto-grants-1985_12 |