huagongshe.com
HRID637303

反应详情

EQUATION

反应方程式

HRID 637303 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1ccc(-n2ccnc2)cc1
HCID736529

4-(1H-Imidazol-1-yl)benzoic acid

C10H8N2O2

结构：CCc1[nH]c(=O)[nH]c1C(=O)O
HCID13815989

5-Ethyl-2-oxo-2,3-dihydro-1H-imidazole-4-carboxylic acid

C6H8N2O3

PRODUCTS

生成物

2
结构：O=C=O
HCID280

Carbon dioxide

CO2

结构：CCc1[nH]c(=O)[nH]c1C(=O)c1ccc(-n2ccnc2)cc1
HCID127769

CK 2289

C15H14N4O2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Na+].[OH-]
溶剂HCID14798

Sodium Hydroxide

HNaO

PROCEDURE

实验过程

In a manner similar to that described in Example IA react 5-ethyl-2,3-dihydro-2-oxo-1H-imidazole-4-carboxylic acid and 4-(1H-imidazol-1-yl)benzoic acid, dissolve the crude free base in aqueous sodium hydroxide and reprecipitate with carbon dioxide to produce the title compound.