Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 86740520 | HCID 86740520 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 56622063 | HCID 56622063 | — |
Reaction Steps
A mixture of 410 mg of methoxymethyl (1R,trans,ΔE) 2,2-dimethyl-3-[2-tert.-butoxy-2-methoxy carbonyl-ethenyl]cyclopropane-carboxylate, 8 ml of methanol, 8 ml of acetone and 16 ml of aqueous N hydrochloric acid was stirred at 20° C. for 6 hours and was poured into water. The mixture was extracted with ether and the organic phase was evaporated to dryness under reduced pressure to obtain 300 mg of (1R,trans,ΔE) 2,2-dimethyl-3-[2-tert.-butoxy-2-methoxy carbonyl-ethenyl]cyclopropane-carboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04556666 |
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| Source dataset | uspto-grants-1985_12 |
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| ORD ID | ord-bc3606d19ddf4b8b9da1747d5f220ae0 |
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| Source note | uspto-grants-1985_12 |
|---|
