Lithium Hydroxide → 1-(4-Azidobutyl)cyclopentanecarboxylic acid

HRID 63734Notes

Reaction equation

C[O:2][C:3]([C:5]1([CH2:10][CH2:11][CH2:12][CH2:13][N:14]=[N+:15]=[N-:16])[CH2:9][CH2:8][CH2:7][CH2:6]1)=[O:4].[OH-].[Li+]>>[N:14]([CH2:13][CH2:12][CH2:11][CH2:10][C:5]1([C:3]([OH:4])=[O:2])[CH2:6][CH2:7][CH2:8][CH2:9]1)=[N+:15]=[N-:16]

Participants

Reactant 2

HCID 3939Lithium Hydroxide

HCID 23384160Methyl 1-(4-azidobutyl)cyclopentane-1-carboxylate

Product 1

HCID 226601411-(4-Azidobutyl)cyclopentanecarboxylic acid

Procedure

The title compound was prepared using a similar procedure as described in Example 1, Step 3, starting from 1-[4-azidobutyl]cyclopentanecarboxylic acid methyl ester and lithium hydroxide.

Sources & evidence

ORD record: ord-f7a1350a131c4e32a2c96ed13e1f1285
Source dataset: uspto-grants-2016_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09447035B2

Reaction notes

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