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HRID637504

反应详情

EQUATION

反应方程式

HRID 637504 反应方程式

REACTANTS

反应物

2
N-(2-Aminoethyl)acetamide 分子结构式
HCID66082

N-(2-Aminoethyl)acetamide

C4H10N2O

5-(4-Isocyanatophenyl)pyrazin-2(1H)-one 分子结构式
HCID20208661

5-(4-Isocyanatophenyl)pyrazin-2(1H)-one

C11H7N3O2

PRODUCTS

产物

1
HCID 13853582 分子结构式
HCID13853582

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
Dimethylformamide 分子结构式
溶剂HCID6228

Dimethylformamide

C3H7NO

PROCEDURE

实验过程

In a manner similar to Example 13b, 5-[4-(isocyanato)phenyl]-2(1H)-pyrazinone is reacted with 2-acetamidoethylamine (1 g) in dimethylformamide (5 ml) for 17 hours at room temperature to form the title compound, m.p. 238°-44° C.; δ(DMSO-d6) 1.80 (s, 3H, COCH3), 7.94, 8.08 (2s, 2H, pyrazinone H's).