Sulfuryl chloride → HCID 13558267, compound

Participants

Reaction Steps

Methyl 3-(4-acetylaminomethylphenyl)propionate (5.00 g, 21.25 mmol) was added to a sulfuryl chloride (85 ml) solution of anhydrous aluminum chloride (14.2 g, 106 mmol) at -25° C. Thereafter, the temperature of the mixture was gradually elevated to 5° C., at which temperature the mixture was subjected to reaction under agitation for 24 hours.

Provenance & Evidence