HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 86740541, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 13560321 | HCID 13560321 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86740541 | HCID 86740541 | 77.3% |
Reaction Steps
A mixture of the 5-thione derivative 5c (1.45 gram, 8 mmol) and methyl iodide (1.21 gram, 8.5 mmol) in 100 ml methanol was refluxed for 6 hours. The solvent was evaporated to dryness leaving the hydroiodide salt 6 (2 grams) as a white solid. Melting point 235°-238° C. (recrystallized from absolute ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04557865 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-f066f58688db4afdac34d74fc0563a08 |
| Source note | uspto-grants-1985_12 |