HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 86051412, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | HCID 86739921 | HCID 86739921 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 86051412 | HCID 86051412 | — |
Reaction Steps
Following the procedure of Preparation 1, 2-bromoethyl-3,5-dichlorophenyl ether and isopropyl amine were reacted in refluxing chloroform overnight to yield an oil, the free base of the title compound. Thereafter, a portion of the oil was reacted with ethereal hydrogen chloride to form the hydrochloride salt in 43.4% yield, m.p. 195°-197° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04558155 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-6e185538399e48e6b66a3fb12e003670 |
| Source note | uspto-grants-1985_12 |