HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 131714113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | HCID 20256299 | HCID 20256299 | — |
| Reactant | HCID 22246762 | HCID 22246762 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 131714113 | HCID 131714113 | — |
Reaction Steps
Following the procedure of Preparation 1, a mixture of 3-[3,5-dichlorophenoxy]-1-chloropropane and 3-[3,5-dichlorophenoxy]-1-bromopropane and isopropyl amine were reacted in refluxing chloroform overnight and the reaction mixture processed to yield an oil, the free base of the title compound. A portion of the oil was reacted with ethereal hydrogen chloride to form the hydrochloride salt; m.p. 157°-159° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04558155 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-ae3fac0fb0b543e3a06771fb01bfb2f1 |
| Source note | uspto-grants-1985_12 |