HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 20256305, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | HCID 86739923 | HCID 86739923 | — |
| Product | HCID 20256305 | HCID 20256305 | — |
Reaction Steps
Following the procedure of Example 11, 2-bromoethyl-2-chlorophenyl ether was reacted with isopropyl amine (excess) and the reaction mixture processed to give an oil, the free base of the title compound. A portion of the oil was reacted with ethereal hydrogen chloride and the hydrochloride salt recrystallized from methanol-diethyl ether, m.p. 118°-119.5° C. (75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04558155 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-c6bcdc7610a54f9db6ee91ea61058637 |
| Source note | uspto-grants-1985_12 |