Hydrochloric Acid → HCID 20256410, compound

HRID 637848Notes

Reaction equation

[Cl:1][C:2]1[CH:3]=[C:4]([CH:9]=[C:10]([Cl:12])[CH:11]=1)[O:5][CH2:6][CH2:7]Br.[CH2:13]([NH2:17])[CH:14]([CH3:16])[CH3:15].Cl>>[ClH:1].[Cl:1][C:2]1[CH:3]=[C:4]([CH:9]=[C:10]([Cl:12])[CH:11]=1)[O:5][CH2:6][CH2:7][NH:17][CH2:13][CH:14]([CH3:16])[CH3:15]

Participants

Reactant 3

HCID 313Hydrochloric Acid

HCID 6558Isobutylamine

HCID 222467761-(2-Bromoethoxy)-3,5-dichlorobenzene

Product 1

HCID 20256410HCID 20256410, compound

Procedure

The title compound was prepared by the method of Preparation 34 from 2-(3,5-dichlorophenoxy)-1-bromoethane and isobutylamine (72 hr) and hydrogen chloride. The free base was obtained as an oil. The hydrochloride salt melted at 190°-191.5° C.

Workup

customThe free base was obtained as an oil

Sources & evidence

ORD record: ord-de67f6f2d39944e49d1d26bbfbdff060
Source dataset: uspto-grants-1985_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04558155

Reaction notes

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