Acetyl chloride → HCID 20256343, compound

HRID 637858Notes

Reaction equation

HRID 637858 reaction equation
[CH3:1][CH:2]([N:4]([CH2:8][CH2:9][O:10][C:11]1[CH:16]=[CH:15][C:14]([NH2:17])=[CH:13][CH:12]=1)[C:5]([NH2:7])=[O:6])[CH3:3].[C:18](Cl)(=[O:20])[CH3:19]>C(N(CC)CC)C>[CH3:5][N:4]([CH3:8])[CH2:2][CH2:1][NH:7][C:5](=[O:6])[N:4]([CH:2]([CH3:1])[CH3:3])[CH2:8][CH2:9][O:10][C:11]1[CH:12]=[CH:13][C:14]([NH:17][C:18](=[O:20])[CH3:19])=[CH:15][CH:16]=1

Participants

4

Reactant 2

HCID 6367Acetyl chlorideHCID 86739924HCID 86739924, compound

Product 1

HCID 20256343HCID 20256343, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The title compound is prepared by reacting the compound of Example 64: N'-[2-dimethylamino)ethyl]-N-(1-methylethyl)-N-[2-(4-aminophenoxy)ethyl]urea with acetyl chloride in triethylamine.

Sources & evidence

ORD record
ord-9d940129e62b4f2ab34a9153616afe4e
Source dataset
uspto-grants-1985_12
Patent number
US04558155

Reaction notes

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