HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetone → HCID 3041219, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetone | HCID 6571 | — |
| Reactant | Semicarbazide hydrochloride | HCID 11236 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 3041219 | HCID 3041219 | — |
Reaction Steps
Add 1.0 gm chloroacetone and a solution of 0.84 gm NaHCO3 in 10 ml water to a solution of 1.1 gm semicarbazide hydrochloride in 25 ml THF and stir overnight. Two layers form. Separate the top layer and concentrate to obtain an off-white solid, 2-semicarbazono-1-chloropropane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04559333 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-0888216fb9a84cc985b2636845a58eb5 |
| Source note | uspto-grants-1985_12 |