HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20255139, compound → HCID 20255123, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20255139 | HCID 20255139 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20255123 | HCID 20255123 | — |
Reaction Steps
A solution of 0.85 g of crude 1-[N-benzyl-2-(3-carbamoyl-4-benzyloxyphenoxy)-ethylamino]-3-[4-[1-methyl-1H-imidazol-2-yl]-phenoxy]-2-propanol in 10 ml of methanol is hydrogenated analogously to Example 8. After working up, the 1-[2-(3-carbamoyl-4-hydroxyphenoxy)-ethylamino]-3-[4-(1-methyl-1H-imidazol-2-yl)-phenoxy]-2-propanol having a melting point of 108°-112° is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04559354 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-77e27092751f47c2aaaa198503beabb4 |
| Source note | uspto-grants-1985_12 |