HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Methionine → HCID 136041194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Methionine | HCID 6137 | — |
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 20255192 | HCID 20255192 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 136041194 | HCID 136041194 | — |
Reaction Steps
Analogously to Example (15b), a mixture of 49.6 g of 1-methyl-3-methylthio-5-(4-methoxyphenyl)-1H-1,2,4-triazole, 40 g of L-methionine and 380 ml of methanesulphonic acid is heated for 24 hours in a bath at 110°-120° and analogously worked up, yielding 5-(4-hydroxyphenyl)-1-methyl-3-methylthio-1H-1,2,4-triazole having a melting point of 216°-220° (from isopropanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04559354 |
| Source dataset | uspto-grants-1985_12 |
| ORD ID | ord-85266e82548740f88bc003124e44c9af |
| Source note | uspto-grants-1985_12 |